鐘離君柏墓出土彩繪陶器顏料的光譜分析

摘要：利用拉曼光譜結合X射線衍射物相檢測方法,對安徽蚌埠雙墩春秋中晚期鐘離君柏墓出土彩繪陶器顏料的物相結構進行了分析測定.結果表明,陶器表面的紅色、黃色和黑色顏料皆保存較好,未發(fā)生明顯變化,分別是無機礦物朱砂(HgS)和針鐵礦(α-FeO(OH))及炭黑.同時,拉曼光譜與X射線衍射分析的結果都顯示紅色顏料朱砂的組成物相單一,不含天然朱砂的伴生礦物石英,且其晶粒尺寸可能在納米范圍,應是由人工合成或經(jīng)過古人的加工、純化處理.針鐵礦的發(fā)現(xiàn)表明春秋時期該礦物己被用作黃色顏料,這是目前己知的針鐵礦作為黃顏料使用的最早的實例.Abstract：Based on the analysis of Raman spectroscopy and XRD methods, the structures of different pigments on the painted pottery from the Monarch Bai Tomb of Zhongli State in the middle and late Spring and Autumn period at Shungdun Village, Bengbu City, Anhui Province were analyzed. The result shows that all the pigments, including red, yellow and black pigments, have been well preserved, and these three pigments were identified as cinnabar, goethite and carbon black respectively. Both Raman spectroscopy and XRD analysis show that the crystal composition of red pigments, cinnabar, is very pure without quartz crystal, the associated crystal of natural cinnabar, and at the same time the crystal size of cinnabar is possibly at the nanometer scale It suggests that this red pigments perhaps were a synthetic material or processed and purified by our ancestors. The dis-covery of goethite shows that this mineral has been used as pigments as early as in the Spring and Autumn period. This is the earliest example that goethite was used as yellow pigments. 作者： 楊玉璋[1]  張居中[1]  左健[2]  闞緒杭[3]  周群[3] Author： YANG Yu-zhang[1]  ZHANG Ju-zhong[1]  ZUO Jian[2]  KAN Xu-hang[3]  ZHOU Qun[3] 作者單位： 中國科學技術大學科技史與科技考古系,安徽,合肥,230026中國科學技術大學合肥微尺度物質科學國家實驗室(籌),安徽,合肥,230026安徽省文物考古研究所,安徽,合肥,230061 期 刊： 光譜學與光譜分析   ISTICEISCIPKU Journal： SPECTROSCOPY AND SPECTRAL ANALYSIS 年，卷(期)： 2010, 30(4) 分類號： P575.4 K876.3 關鍵詞： 彩繪陶    顏料    拉曼光譜    X射線衍射    Keywords： Painted pottery    Pigments    Raman spectroscopy    XRD    機標分類號： TQ1 O41 機標關鍵詞： 出土    彩繪    陶器顏料    光譜分析    Spring and Autumn period    Raman spectroscopy    針鐵礦    射線衍射    拉曼光譜    analysis    nanometer scale    quartz crystal    black pigments    朱砂    物相    礦物    yellow    crystal size    carbon black    春秋中晚期 基金項目： 國家自然科學基金，中國科學院科研啟動專項資金項目 鐘離君柏墓出土彩繪陶器顏料的光譜分析[期刊論文]  光譜學與光譜分析 --2010, 30(4)楊玉璋  張居中  左健  闞緒杭  周群利用拉曼光譜結合X射線衍射物相檢測方法,對安徽蚌埠雙墩春秋中晚期鐘離君柏墓出土彩繪陶器顏料的物相結構進行了分析測定.結果表明,陶器表面的紅色、黃色和黑色顏料皆保存較好,未發(fā)生明顯變化,分別是無機礦物朱砂(HgS...

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